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Even if your management does not understand the value of the services you provide to the organization, they will usually understand the value when it is presented as a thick stack of documentation Make sure that documentation is stored on paper too If the system is down when you need the manuals, you re not going to be able to get to them Keep them in binders so that they can be easily changed and updated After the documentation is written, don t forget to review it and update it on a regular basis Bad documentation is worse than none at all In a crisis, especially if the most knowledgeable people are not around, documentation is likely to be followed verbatim If it s wrong, things can go from bad to worse A common question about preparing documentation is at what technical level it should be written.

Here, we introduce the more broadly used gures of merit with their generally accepted de nitions Basic statistical procedures are also presented More technical sources of further information are offered in the Suggested Reading section Bioanalytical methods are classi ed according to the kind of results they provide Qualitative assays provide information about the presence or absence of the analyte, whereas quantitative assays give the analyte concentration and the uncertainty in this value, in the sample Semiquantitative methods give an estimate of concentration and are used to determine whether analyte is present at a level that is above or below a reference concentration; therefore the report can state if the concentration in the sample is higher, similar, or lower than the reference value 162 PRECISION AND ACCURACY Uncertainty is classi ed in two major groups: Random error is always present in experimental data and can never be completely eliminated.

One school of thought says that documentation should be written so that anyone in the organization, from a janitor to the CEO, can follow it and, if required, bring the systems up after a disaster After all, the system administrative staff may not be available at the time, and someone has to do it While that is a noble goal, it is an impractical one The state of the critical systems changes all the time The more detail that is included.

Security: the service infrastructure must manage the service access policy, both for internal calls to the information system and for external calls from partners Global management: the infrastructure must provide functions for managing deployment as well as versions of services, plus mediation processes, exchange processes, and business processes It must also offer the complete set of services registry mechanisms for managing the lifecycle for these services: in development, in production, etc Finally, it must supply all the functionalities for managing access authorization to the various functions that it provides Supervision: the infrastructure must provide functions for constructing performance indicators and tracking dashboards on the use of services and on the associated business activity We could note that the functionalities described above are part of the servicelevel integration required for implementing an integration infrastructure, such as is described in 3 They are not all necessarily present in the different tools.

It can result from the random nature of collisions that lead to chemical or biochemical reactions, or may be caused by small voltage uctuations in measurement instrumentation Random error causes positive and negative deviations from the true value, and affects the precision of the results Precision is usually discussed in terms of standard deviation (s) and relative standard deviation (RSD), both de ned later in this chapter Systematic error is produced by a more or less constant mistake, and results in a.

5